Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(4-nitrophenyl)pentanamide → N-(4-aminophenyl)pentanamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(4-nitrophenyl)pentanamide | HCID 3762929 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | N-(4-aminophenyl)pentanamide | HCID 1725711 | — |
반응 단계
A solution of 4'-nitrovaleranilide (13.33 g., 0.06 mole) in absolute ethanol (750 ml.) is hydrogenated over 10% palladium on charcoal (2 g.) until the theoretical absorption is achieved. The catalyst is removed and the solvent is removed in vacuo. The residue is recrystallized from butyl chloride to yield 9.0 g., m.p. 81°-83° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04006233 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-8c20ac76b3604360b3c9fcffec14b3fe |
| 출처 메모 | uspto-grants-1977_02 |