Potassium Iodide → HCID 70605999, 화합물

HRID 435852

반응식

HRID 435852 반응식
[CH2:1]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1O)[CH2:2][CH2:3][CH3:4].Br[CH2:13][CH2:14][CH2:15][Br:16].[C:17](=[O:20])([O-])[O-].[K+].[K+].[I-].[K+]>CC(C)=O>[Br:16][CH2:15][CH2:14][CH2:13][C:6]1[C:5]([CH2:1][CH2:2][CH2:3][CH3:4])=[C:10]([O:20][C:17]2[CH:3]=[CH:2][CH:1]=[C:5]([CH2:13][CH2:14][CH2:15][Br:16])[C:6]=2[CH2:7][CH2:8][CH2:9][CH3:10])[CH:9]=[CH:8][CH:7]=1

참가 물질

6

반응물 4

HCID 4875Potassium IodideHCID 80011,3-DibromopropaneHCID 11430Potassium CarbonateHCID 185152-Butylphenol

생성물 1

HCID 70605999HCID 70605999, 화합물

시약·촉매·용매 1

HCID 180Acetone용매2회

실험 절차

A solution of 30 parts of o-n-butylphenol in 150 parts of dry acetone was added dropwise over 5 hours to a stirred refluxing suspension of 80.8 parts of 1,3-dibromopropane, 27.6 parts of anydrous potassium carbonate and 0.5 parts of potassium iodide in 170 parts of dry acetone.

후처리

  1. temperaturerefluxing

출처 및 근거

ORD 기록
ord-39881e86d69d4ff0ae052c49ca3dda0b
출처 데이터셋
uspto-grants-1977_02
특허 번호
US04006245

연결된 노트

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