Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formic Acid → N-(3-(dimethylamino)propyl)formamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formic Acid | HCID 284 | — |
| 반응물 | Toluene | HCID 1140 | — |
| 반응물 | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-(3-(dimethylamino)propyl)formamide | HCID 80020 | 59% |
반응 단계
Formic acid (23 g., 0.5 mole), dimethylaminopropylamine (51 g., 0.5 mole) and toluene (50 ml) were azeotroped together with continual removal of water using a Dean and Stark separator until no more water was formed. Toluene was distilled off and the pale yellow residue distilled in vacuo. The colourless liquid product of low smell (N-(3-dimethylaminopropyl)formamide) was obtained in a yield of 59% of theory, b.p. 140° C/15 mm Hg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04007140 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-e537d7b8b53e40359f2afc800bf1e2f2 |
| 출처 메모 | uspto-grants-1977_02 |