Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Azide → 3-Aminorifamycin S
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Azide | HCID 33557 | — |
| 반응물 | Rifamycin S | HCID 6436726 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 3-Aminorifamycin S | HCID 12889622 | 25.5% |
반응 단계
50 g rifamycin S were dissolved in 200 ml dimethyl formamide and added with 9 g sodium azide. After 36 hours at a temperature of +5° C, the reaction mixture was treated as in Example 3, to obtain 13 g 3-amino-rifamycin S identical to that described in Example 3.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04007169 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-f05fa6bfaf3840458238356cf61f0acd |
| 출처 메모 | uspto-grants-1977_02 |