Isobutylamine → HCID 12671199, 화합물
반응식
Cl[C:2]1[N:7]2[N:8]=[CH:9][N:10]=[C:6]2[N:5]=[C:4]([CH3:11])[C:3]=1[CH2:12][CH2:13]Cl.[CH2:15]([NH2:19])[CH:16]([CH3:18])[CH3:17].C(=O)([O-])[O-].[Na+].[Na+]>C(O)C>[CH2:15]([N:19]1[C:2]2[N:7]3[N:8]=[CH:9][N:10]=[C:6]3[N:5]=[C:4]([CH3:11])[C:3]=2[CH2:12][CH2:13]1)[CH:16]([CH3:18])[CH3:17]참가 물질
5
실험 절차
A mixture of 2.3g of 7-chloro-6-(2-chloroethyl)-5-methyl-s-triazolo[1,5-a]pyrimidine, 1g of isobutylamine, 1.8g of sodium carbonate and 20 ml of ethanol was treated by the same manner as described in Example 3. The crystals thus obtained were recrystallized from aqueous methanol to give 1.4g of pale yellow prisms of m.p. 143° - 145° C.
후처리
- additionwas treated by the same manner
- customThe crystals thus obtained
- customwere recrystallized from aqueous methanol
출처 및 근거
- ORD 기록
- ord-96bae4cf2edb4213b8309f74aeed415b
- 출처 데이터셋
- uspto-grants-1977_02
- 특허 번호
- US04007189
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