Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl Benzoin → Cinnamyl methacrylate 1-naphthyl methacrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl Benzoin | HCID 98097 | — |
| 반응물 | Cinnamyl methacrylate | HCID 228230 | — |
| 반응물 | Naphthyl methacrylate | HCID 4064248 | — |
| 반응물 | Nitrosocyclohexane | HCID 11768540 | — |
| 반응물 | p-Xylylene diacrylate | HCID 11961420 | — |
| 용매 | Benzene | HCID 241 | — |
| 용매 | 1-Chloronaphthalene | HCID 7003 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | Cinnamyl methacrylate 1-naphthyl methacrylate | HCID 86734496 | — |
반응 단계
A mixture of 2.00 g poly(cinnamyl methacrylate/-1-naphthyl methacrylate), 1.50 g 1-naphthyl methacrylate, 0.25 g p-xylylene diacrylate, 0.40 g benzoin methyl ether, 0.05 g 20% nitrosocyclohexane dimer in 1-chloronaphthalene, and 3.00 g xylene was prepared. Poly(cinnamyl methacrylate/1-naphthyl methacrylate) was prepared by thermally copolymerizing equal parts of cinnamyl methacrylate and 1-naphthyl methacrylate in a benzene solution using an azonitrile initiator. The polymer was precipitated from solution and washed prior to use.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04008083 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-9a576419313945b99d3a9a36026ccab0 |
| 출처 메모 | uspto-grants-1977_02 |