Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylene blue cation → Anthracene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylene blue cation | HCID 4139 | — |
| 반응물 | Rose Bengal Lactone | HCID 69439 | — |
| 생성물 | Anthracene | HCID 8418 | — |
반응 단계
(8.3 mmol) and 500 mg. of photosensitizing resin were mixed in 100 ml. of chloroform and irradiated. After 148 cc. (6.6 mmol) of oxygen was absorbed the resin was filtered off, the solution was decolorised with charcoal and evaporated to dryness. The residue was fractionally recrystallized from chloroform to yield anthracene endoperoxide, mp 137°-143°. Rose bengal attached to IRA-400 and methylene blue attached to IRC-200 both gave the same results.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04008136 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-8450af46488242d799e4407a346031bb |
| 출처 메모 | uspto-grants-1977_02 |