Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Carbon Disulfide → Triethylammonium 2-Trichloromethyl-3-oxazolidinecarbodithioate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Carbon Disulfide | HCID 6348 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 2-(Trichloromethyl)oxazolidine | HCID 99029 | — |
| 생성물 | Triethylammonium 2-Trichloromethyl-3-oxazolidinecarbodithioate | HCID 22766662 | — |
반응 단계
A mixture of 114 g (0.60 mole) 2-trichloromethyloxazolidine, 121.2g. (1.2 moles) triethylamine and 68.4 g. (0.9 mole) carbon disulfide was heated at 50° for 7 hours and then was left standing for 18 hours at room temperature. The yellow solids were filtered, stirred with anhydrous ethyl ether, and filtered again to obtain 195.5 g (88.7% conversion) of the desired product, m.p. 107°-110° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04008244 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-03c5ee330ff449fcb8297588d418eeb9 |
| 출처 메모 | uspto-grants-1977_02 |