Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Boron trifluoride → Dilauryl Ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Boron trifluoride | HCID 6356 | — |
| 반응물 | Epichlorohydrin | HCID 7835 | — |
| 반응물 | 1-Dodecanol | HCID 8193 | — |
| 생성물 | Dilauryl Ether | HCID 20667 | — |
| 생성물 | (Z)-3-chloroprop-1-en-1-ol | HCID 15676292 | — |
반응 단계
185 g of glycerol epichlorhydrin are reacted with one mole, i.e., 186 g of dodecanol at 75-80° C in the presence of 1.5 ml of an acetic acid complex containing 36% BF3. Dodecyl ether of polyepichlorohydrin having the following formula is obtained:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04009255 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-ed296078d4924863935e1c4532039c27 |
| 출처 메모 | uspto-grants-1977_02 |