Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Hydroxide → N,N'-Heptamethylenebis(4-isopropoxybenzamide)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 1,7-Heptanediamine | HCID 69533 | — |
| 반응물 | 4-Isopropoxybenzoyl chloride | HCID 2724465 | — |
| 용매 | 1,2-Dichloroethane | HCID 11 | — |
| 생성물 | N,N'-Heptamethylenebis(4-isopropoxybenzamide) | HCID 21452919 | — |
반응 단계
m.p. 135°-136° C., 10.9 g., was prepared as in Example 1 using a solution of 4-isopropoxybenzoyl chloride (from 18.0 g. of 4-isopropoxybenzoic acid as in Example 6) in 100 ml. of ethylene dichloride, 8.9 g. of 1,7-heptanediamine, 200 ml. of 10% aqueous potassium hydroxide solution, 500 ml. ethylene dichloride and recrystallization from acetonitrile using decolorizing charcoal.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04009208 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-91a8fc79e8c046b988e192deb662d36c |
| 출처 메모 | uspto-grants-1977_02 |