Potassium Hydroxide → HCID 21452919, 화합물

HRID 436634

반응식

HRID 436634 반응식
[CH:1]([O:4][C:5]1[CH:13]=[CH:12][C:8]([C:9](Cl)=[O:10])=[CH:7][CH:6]=1)([CH3:3])[CH3:2].[CH2:14]([NH2:22])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][NH2:21].[OH-:23].[K+]>C(Cl)CCl>[CH:1]([O:4][C:5]1[CH:13]=[CH:12][C:8]([C:9]([NH:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][NH:22][C:9](=[O:10])[C:8]2[CH:12]=[CH:13][C:5]([O:23][CH:1]([CH3:2])[CH3:3])=[CH:6][CH:7]=2)=[O:10])=[CH:7][CH:6]=1)([CH3:3])[CH3:2]

참가 물질

5

반응물 3

HCID 14797Potassium HydroxideHCID 695331,7-HeptanediamineHCID 27244654-Isopropoxybenzoyl chloride

생성물 1

HCID 21452919HCID 21452919, 화합물

시약·촉매·용매 1

HCID 111,2-Dichloroethane용매

실험 절차

m.p. 135°-136° C., 10.9 g., was prepared as in Example 1 using a solution of 4-isopropoxybenzoyl chloride (from 18.0 g. of 4-isopropoxybenzoic acid as in Example 6) in 100 ml. of ethylene dichloride, 8.9 g. of 1,7-heptanediamine, 200 ml. of 10% aqueous potassium hydroxide solution, 500 ml. ethylene dichloride and recrystallization from acetonitrile using decolorizing charcoal.

후처리

  1. customethylene dichloride and recrystallization from acetonitrile using

출처 및 근거

ORD 기록
ord-91a8fc79e8c046b988e192deb662d36c
출처 데이터셋
uspto-grants-1977_02
특허 번호
US04009208

연결된 노트

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