Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Hydroxide → N,N'-Dodecamethylenebis(4-trifluoromethoxybenzamide)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 1,12-Dodecanediamine | HCID 17727 | — |
| 반응물 | 4-(Trifluoromethoxy)benzoyl Chloride | HCID 142110 | — |
| 용매 | 1,2-Dichloroethane | HCID 11 | — |
| 생성물 | N,N'-Dodecamethylenebis(4-trifluoromethoxybenzamide) | HCID 21452860 | — |
반응 단계
m.p. 158°-159° C., 11.3 g., was prepared as in Example 1 using 24.8 g. of 4-trifluoromethoxybenzoyl chloride in 150 ml. of ethylene dichloride, 10.0 g. of 1,12-dodecanediamine, 60 ml. of 10% aqueous potassium hydroxide solution, 350 ml. of ethylene dichloride and recrystallization twice from ethanol and once from isopropyl alcohol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04009208 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-dcc3d143b4c94612acec4c4e25b57104 |
| 출처 메모 | uspto-grants-1977_02 |