Nitric Acid → m-Nitrobenzenephosphonous acid

HRID 436906노트

반응식

HRID 436906 반응식
[C:1]1([P:7]([OH:9])[OH:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.S(=O)(=O)(O)O.[N+:15]([O-])([OH:17])=[O:16]>>[N+:15]([C:3]1[CH:2]=[C:1]([P:7]([OH:9])[OH:8])[CH:6]=[CH:5][CH:4]=1)([O-:17])=[O:16]

참가 물질

4

반응물 3

HCID 944Nitric AcidHCID 1118Sulfuric AcidHCID 72903Phenylphosphinic acid

생성물 1

HCID 21431775m-Nitrobenzenephosphonous acid

실험 절차

reacting benzenephosphonous acid in a sulfuric acid medium under nitrating conditions by the dropwise addition of nitric acid at a temperature of about 0° C. to about 5° C. to form m-nitrobenzenephosphonous acid in a reaction mixture;

출처 및 근거

ORD 기록
ord-14b9c7d9ecd64990bf6cc490b8bde3a2
출처 데이터셋
uspto-grants-1977_06
특허 번호
US04028403

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