Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N,N-Dimethylallylamine → Allyl n-butoxymethyl dimethylammonium chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N,N-Dimethylallylamine | HCID 75082 | — |
| 반응물 | 1-(Chloromethoxy)butane | HCID 11105357 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | Allyl n-butoxymethyl dimethylammonium chloride | HCID 21429949 | — |
반응 단계
24.7 grams of chloromethyl butyl ether was added to 17 grams of allyl dimethylamine in 32 grams of ethyl acetate. The reaction was highly exothermic and two layers formed very rapidly. Stirring was continued at 25° C. for 24 hours, after which the solvent was removed by vacuum. Chloride analysis of the rather viscous liquid product indicated 91% of theoretical.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04029658 |
| 출처 데이터셋 | uspto-grants-1977_06 |
| ORD ID | ord-555e2f750b504c65a2b53b679bcae8c9 |
| 출처 메모 | uspto-grants-1977_06 |