Diethyl Ether → 1-Phenethyl-4-acetamidopyridinium bromide

HRID 437232

반응식

HRID 437232 반응식
[CH2:1]([Br:9])[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:10]([NH:13][C:14]1[CH:19]=[CH:18][N:17]=[CH:16][CH:15]=1)(=[O:12])[CH3:11].CCOCC>C(O)C>[Br-:9].[CH2:1]([N+:17]1[CH:18]=[CH:19][C:14]([NH:13][C:10](=[O:12])[CH3:11])=[CH:15][CH:16]=1)[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

참가 물질

5

반응물 3

HCID 3283Diethyl EtherHCID 7666Phenethyl bromideHCID 21288N-Pyridin-4-ylacetamide

생성물 1

HCID 214305751-Phenethyl-4-acetamidopyridinium bromide

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A solution of phenethyl bromide and 4-acetamidopyridine in absolute ethanol was heated under reflux, cooled, treated with ether and allowed to stand overnight to give 1-phenethyl-4-acetamidopyridinium bromide.

후처리

  1. temperatureunder reflux
  2. temperaturecooled

출처 및 근거

ORD 기록
ord-214c2e88460b4e1294f116b5943c8030
출처 데이터셋
uspto-grants-1977_06
특허 번호
US04029801

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