Toluene → HCID 21428717, 화합물

HRID 437579노트

반응식

HRID 437579 반응식
C([N:8]1[CH2:13][CH2:12][C:11]([C:25]2[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=2)([O:14][C:15]2[CH:20]=[CH:19][C:18]([C:21]([F:24])([F:23])[F:22])=[CH:17][CH:16]=2)[CH2:10][CH2:9]1)C1C=CC=CC=1.[C:31]1([O:37][C:38](Cl)=[O:39])[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1.C1(C)C=CC=CC=1>CCCCCC>[O:37]([C:38]([N:8]1[CH2:9][CH2:10][C:11]([C:25]2[CH:26]=[CH:27][CH:28]=[CH:29][CH:30]=2)([O:14][C:15]2[CH:16]=[CH:17][C:18]([C:21]([F:22])([F:23])[F:24])=[CH:19][CH:20]=2)[CH2:12][CH2:13]1)=[O:39])[C:31]1[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1

참가 물질

5

반응물 3

HCID 1140TolueneHCID 15891Phenyl chloroformateHCID 214287034-Phenyl-1-(phenylmethyl)-4-[4-(trifluoromethyl)phenoxy]piperidine

생성물 1

HCID 21428717HCID 21428717, 화합물

시약·촉매·용매 1

HCID 8058Hexane용매

실험 절차

A solution of 10.0 g of 1-benzyl-4-phenyl-4-(p-trifluoromethylphenoxy)piperidine and 4.1 g of phenylchloroformate in 100 ml. of toluene was refluxed for 17 hours. The toluene was removed under reduced pressure to give a colorless oil which when rubbed with a glass rod in the presence of hexane gave a white solid of 1-phenoxycarbonyl-4-phenyl-4-(p-trifluoromethylphenoxy)piperidine.

후처리

  1. customThe toluene was removed under reduced pressure
  2. customto give a colorless oil which when

출처 및 근거

ORD 기록
ord-bdcd67b513d74288afbc06b08fb64a16
출처 데이터셋
uspto-grants-1977_06
특허 번호
US04031221

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