Methane → 2-(6-Carboxyhexyl)benzyl alcohol

HRID 437987

반응식

HRID 437987 반응식
[C:1]([OH:9])(=[O:8])[CH:2]=[CH:3][CH2:4][CH2:5][CH2:6][CH3:7].[CH4:10]>C(O)C>[C:1]([CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:10]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[CH2:1][OH:8])([OH:9])=[O:8]

참가 물질

4

반응물 2

HCID 297MethaneHCID 29373Heptenoic acid

생성물 1

HCID 539714442-(6-Carboxyhexyl)benzyl alcohol

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A solution of 2.30 g. of the above heptenoic acid in 100 ml. of ethanol is stirred with 5 g. of activated charcoal for 30 minutes and filtered. The filtrate is hydrogenated at atmospheric pressure in the presence of 143 mg. of platinum oxide. The solution is filtered, evaporated and recrystallized from toluene to yield 2-(6-carboxyhexyl)benzyl alcohol as white crystals having a melting point of 75°-77° C.

후처리

  1. filtrationfiltered
  2. filtrationThe solution is filtered
  3. customevaporated
  4. customrecrystallized from toluene

출처 및 근거

ORD 기록
ord-a434d3d6d1b8480e8bb79ac2a2025f06
출처 데이터셋
uspto-grants-1977_06
특허 번호
US04032656

연결된 노트

불러오는 중…