참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Phosphoric Acid | HCID 1004 | — |
| 반응물 | Tetramethylammonium hydroxide | HCID 60966 | — |
| 반응물 | Titanium oxide (Ti3O) | HCID 162651 | — |
| 생성물 | Tetramethylammonium | HCID 6380 | — |
| 생성물 | Phosphoric acid, titanium(4+) salt (4:3) | HCID 159761 | — |
반응 단계
0.05 mol of tetramethylammonium hydroxide (N(CH3)4OH) in aqueous solution was mixed with 0.15 mol of orthophosphoric acid (H3PO4). Then 0.05 mol of titanium dioxide in the anatase form (i.e., native TiO2) was added to the reaction mixture. After thorough mixing, the mixture was sealed inside a pressure reactor at 6~7 atm and heated in an oven at 180° C. for three days. After cooling, rinsing, filtration, and drying, a tetramethylammonium form of layered titanium phosphate (NMe4TP) was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05514490 |
|---|
| 출처 데이터셋 | uspto-grants-1996_05 |
|---|
| ORD ID | ord-ede9e910bc3d42f199ed34b2e7fb4ec1 |
|---|
| 출처 메모 | uspto-grants-1996_05 |
|---|
