돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 439631생성일: 2026년 10월 25일

4-(4-Phenyl-4-n-propyl-4-silacyclohexyl)cyclohexanone → 4-(4-(4-Fluorophenyl)-3-cyclohexenyl)-1-phenyl-1-n-propyl-1-silacyclohexane

https://huagongshe.com/reaction/439631

반응식

참여 물질

역할이름HCID투입량
반응물4-(4-Phenyl-4-n-propyl-4-silacyclohexyl)cyclohexanoneHCID 11034390—
반응물HCID 178505844HCID 178505844—
생성물4-(4-(4-Fluorophenyl)-3-cyclohexenyl)-1-phenyl-1-n-propyl-1-silacyclohexaneHCID 1101469482%

반응 단계

In the same manner as in Example 1, 35.0 g of 4-(4-n-propyl-4-phenyl-4-silacyclohexyl)cyclohexanone were subjected to coupling reaction with 4-fluorophenylmagnesium chloride, followed by dehydration reaction in the presence of an acid catalyst to obtain 35.9 g of 4-(4-n-propyl-4-phenyl-4-silacyclohexyl)-1-(4-fluorophenyl)-1-cyclohexene (yield: 82%). The results of 1H-NMR analysis are shown below. 1H-NMR (CDCl3) δ:0.50-2.55 (23H, m), 5.90-6.14 (1H, m), 6.80-7.65 (9H, ppm

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05514824
출처 데이터셋uspto-grants-1996_05
ORD IDord-c1ad0bce64464ad4b2e00e75591c42e0
출처 메모uspto-grants-1996_05