4-(4-(3-Methylbutyl)-4-phenyl-4-silacyclohexyl)cyclohexanone → HCID 178447723, 화합물

HRID 439632

반응식

HRID 439632 반응식
[CH3:1][CH:2]([CH3:24])[CH2:3][CH2:4][Si:5]1(C2C=CC=CC=2)[CH2:10][CH2:9][CH:8]([CH:11]2[CH2:16][CH2:15][C:14](=O)[CH2:13][CH2:12]2)[CH2:7][CH2:6]1.[F:25][C:26]1[CH:27]=[C:28]([Mg]Br)[CH:29]=[CH:30][C:31]=1[F:32]>>[CH3:24][CH:2]([CH3:1])[CH2:3][CH2:4][Si@H:5]1[CH2:6][CH2:7][C@H:8]([C:11]2[CH:12]=[CH:13][C:14]([C:29]3[CH:28]=[CH:27][C:26]([F:25])=[C:31]([F:32])[CH:30]=3)=[CH:15][CH:16]=2)[CH2:9][CH2:10]1

참가 물질

3

반응물 2

HCID 214703124-(4-(3-Methylbutyl)-4-phenyl-4-silacyclohexyl)cyclohexanoneHCID 178505835HCID 178505835, 화합물

생성물 1

HCID 178447723HCID 178447723, 화합물

실험 절차

The general procedure of Example 12 was repeated using 34.3 g of 4-(4-(3-methylbutyl)-4-phenyl-4-silacyclohexyl)cyclohexanone and 3,4-difluorophenylmagnesium bromide, thereby obtaining the captioned compound.

후처리

  1. customobtaining the captioned compound

출처 및 근거

ORD 기록
ord-917ac78deb614f2ab7f63f4dfc1f9b32
출처 데이터셋
uspto-grants-1996_05
특허 번호
US05514824

연결된 노트

불러오는 중…