4-(4-(3-Methoxypropyl)-4-phenyl-4-silacyclohexyl)cyclohexanone → HCID 178495606, 화합물

HRID 439633

반응식

HRID 439633 반응식
[CH3:1][O:2][CH2:3][CH2:4][CH2:5][Si:6]1(C2C=CC=CC=2)[CH2:11][CH2:10][CH:9]([CH:12]2[CH2:17][CH2:16][C:15](=O)[CH2:14][CH2:13]2)[CH2:8][CH2:7]1.[F:25][C:26]1[CH:27]=[C:28]([Mg]Br)[CH:29]=[CH:30][C:31]=1[F:32]>>[CH3:1][O:2][CH2:3][CH2:4][CH2:5][Si@H:6]1[CH2:7][CH2:8][C@H:9]([C:12]2[CH:13]=[CH:14][C:15]([C:29]3[CH:28]=[CH:27][C:26]([F:25])=[C:31]([F:32])[CH:30]=3)=[CH:16][CH:17]=2)[CH2:10][CH2:11]1

참가 물질

3

반응물 2

HCID 224125064-(4-(3-Methoxypropyl)-4-phenyl-4-silacyclohexyl)cyclohexanoneHCID 178505835HCID 178505835, 화합물

생성물 1

HCID 178495606HCID 178495606, 화합물

실험 절차

The general procedure of Example 12 was repeated using 34.5 g of 4-(4-(3-methoxypropyl)-4-phenyl-4-silacyclohexyl)cyclohexanone and 3,4-difluorophenylmagnesium bromide, thereby obtaining the captioned compound.

후처리

  1. customobtaining the captioned compound

출처 및 근거

ORD 기록
ord-12b32279c1f648aab07b4972075439df
출처 데이터셋
uspto-grants-1996_05
특허 번호
US05514824

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