Oxalyl chloride → 3,4,4-Trifluoro-3-butenoyl chloride

HRID 439666

반응식

HRID 439666 반응식
[F:1][C:2](=[C:7]([F:9])[F:8])[CH2:3][C:4](O)=[O:5].C(Cl)(=O)C([Cl:13])=O>CN(C=O)C>[F:1][C:2](=[C:7]([F:9])[F:8])[CH2:3][C:4]([Cl:13])=[O:5]

참가 물질

4

반응물 2

HCID 65578Oxalyl chlorideHCID 152391743,4,4-Trifluoro-3-butenoic acid

생성물 1

HCID 109207893,4,4-Trifluoro-3-butenoyl chloride

시약·촉매·용매 1

HCID 6228Dimethylformamide촉매

실험 절차

Reaction of 3,4,4-trifluoro-3-butenoic acid (IV) with oxalyl chloride in the presence of DMF as a catalyst without any solvent to give 3,4,4-trifluoro-3-butenoyl chloride (V).

출처 및 근거

ORD 기록
ord-4b00ceea182645f4816f12525188ca9c
출처 데이터셋
uspto-grants-1996_05
특허 번호
US05514717

연결된 노트

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