Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → Benzoic acid, 4-ethyl-, methyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | 4-Ethylbenzoic Acid | HCID 12086 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | Benzoic acid, 4-ethyl-, methyl ester | HCID 23827 | — |
반응 단계
A mixture of 4-ethylbenzoic acid (5.12 g), thionyl chloride (3.0 ml) and methanol (150 ml) was heated and refluxed. After 3 hours, the mixture was concentrated under reduced pressure to give methyl 4-ethylbenzoate (5.59 g). this product was used in the subsequent step without purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05516777 |
| 출처 데이터셋 | uspto-grants-1996_05 |
| ORD ID | ord-cfb03ca1633a47faa484d1cc6cde5262 |
| 출처 메모 | uspto-grants-1996_05 |