Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Bicarbonate → (S)-Benzyl piperidine-2-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 반응물 | Benzyl piperidine-2-carboxylate | HCID 12436232 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | (S)-Benzyl piperidine-2-carboxylate | HCID 12436231 | — |
반응 단계
Benzyl pipecolate was routinely generated by treating an ethyl acetate suspension of this salt with saturated sodium bicarbonate until dissolution of the organic material. The aqueous layer was extracted twice with ethyl acetate and the combined organic extracts were dried with MgSO4 and evaporated to yield (S)-Benzyl pipecolate (133) as a pale yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05516797 |
| 출처 데이터셋 | uspto-grants-1996_05 |
| ORD ID | ord-a1a196c1d37c4c3f9bf2e3b0eeb99535 |
| 출처 메모 | uspto-grants-1996_05 |