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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 440244생성일: 2026년 10월 23일

1-(3-Nitropyridin-2-yl)piperazine → 2-(Piperazin-1-yl)pyridin-3-amine

https://huagongshe.com/ko/reaction/440244

반응식

참여 물질

역할이름HCID투입량
반응물1-(3-Nitropyridin-2-yl)piperazineHCID 3778834—
반응물HCID 178418361HCID 178418361—
촉매HCID 178418390HCID 178418390—
용매MethanolHCID 887—
생성물2-(Piperazin-1-yl)pyridin-3-amineHCID 1039735895.8%

반응 단계

In 30 ml of methanol was dissolved 3.13 g (0.015 mole) of 1-(3-nitro-2-pyridyl)piperazine, and 2 g of 5% palladium carbon was added thereto. While stirring the mixture at room temperature, hydrogen gas was passed through for one hour. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to obtain 2.56 g of 1-(3-amino-2-pyridyl)piperazine as pale yellow liquid.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05519016
출처 데이터셋uspto-grants-1996_05
ORD IDord-ddd5187149e74fe9b7a86c02188a48f5
출처 메모uspto-grants-1996_05