Thionyl Chloride → 1-(2-Methoxyphenyl)cyclopropane-1-carbonyl chloride

HRID 440500노트

반응식

HRID 440500 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[C:9]1([C:12]([OH:14])=O)[CH2:11][CH2:10]1.S(Cl)([Cl:17])=O>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[C:9]1([C:12]([Cl:17])=[O:14])[CH2:11][CH2:10]1

참가 물질

3

반응물 2

HCID 24386Thionyl ChlorideHCID 184000111-(2-Methoxyphenyl)cyclopropane-1-carboxylic acid

생성물 1

HCID 242737911-(2-Methoxyphenyl)cyclopropane-1-carbonyl chloride

실험 절차

1-(2-methoxyphenyl)cyclopropane carboxylic acid (19 g) and thionyl chloride (30 ml) were heated under gentle reflux for 2 hours. The solvent was evaporated to yield 1-(2-methoxyphenyl)cyclopropane carbonyl chloride.

후처리

  1. temperatureunder gentle reflux for 2 hours
  2. customThe solvent was evaporated

출처 및 근거

ORD 기록
ord-9bd963ed53c64b00944548ac86d2f391
출처 데이터셋
uspto-grants-1996_05
특허 번호
US05519034

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