Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Undecanoic Acid → Undecanoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Undecanoic Acid | HCID 8180 | — |
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 촉매 | Dimethylformamide | HCID 6228 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Undecanoyl chloride | HCID 87287 | 39.8% |
반응 단계
Under a nitrogen atmosphere, a solution of 5.0 grams (0.027 mole) of undecanoic acid in 75 mL of methylene chloride was stirred and 2.8 ml (0.032 mole) of oxalyl chloride and 5 drops of N,N-dimethylformamide were added. Upon completion of addition, the reaction mixture was stirred for about 16 hours, then it was concentrated under reduced pressure, yielding 2.2 grams of undecanoyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05521192 |
| 출처 데이터셋 | uspto-grants-1996_05 |
| ORD ID | ord-6e366cb4a7924555947d4f40ba8a8ff0 |
| 출처 메모 | uspto-grants-1996_05 |