Sodium Bicarbonate → HCID 86626532, 화합물

HRID 44156노트

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HRID 44156 반응식
[C:1]([O:8][CH:9]1[CH:14]([CH:15]([CH3:17])[CH3:16])[CH2:13][CH2:12][CH:11]([CH3:18])[CH2:10]1)(=[O:7])[CH2:2][CH2:3][C:4]([O-:6])=[O:5].C(=O)(O)[O-].[Na+:23]>C(O)C>[C:1]([O:8][CH:9]1[CH:14]([CH:15]([CH3:17])[CH3:16])[CH2:13][CH2:12][CH:11]([CH3:18])[CH2:10]1)(=[O:7])[CH2:2][CH2:3][C:4]([O-:6])=[O:5].[Na+:23]

참가 물질

4

반응물 2

HCID 516892Sodium BicarbonateHCID 186766644-{[5-Methyl-2-(propan-2-yl)cyclohexyl]oxy}-4-oxobutanoate2회

생성물 1

HCID 86626532HCID 86626532, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

Monomenthyl succinate (0.5 g, 1.95 mmol) was dissolved in ethanol (6.3 ml). Sodium bicarbonate solution (0.196 g, 2.33 mmol in 10 ml DI H2O) was slowly added to the monomenthyl succinate solution at room temperature. The mixture was stirred for 19 hours. Water and ethanol were removed by rotary evaporator at 50° C., followed by high vacuum line at 50° C. to give sodium monomenthyl succinate as a fine white powder.

후처리

  1. customWater and ethanol were removed by rotary evaporator at 50° C.
  2. customfollowed by high vacuum line at 50° C.

출처 및 근거

ORD 기록
ord-2797674f93f64de495e77f069694f599
출처 데이터셋
uspto-grants-2013_09
특허 번호
US08541401B2

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