Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Bromide → 2-Benzyl-6-methoxyisoquinolinium bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Bromide | HCID 7498 | — |
| 반응물 | 6-Methoxyisoquinoline | HCID 11040978 | — |
| 용매 | Acetone | HCID 180 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 2-Benzyl-6-methoxyisoquinolinium bromide | HCID 21418213 | — |
반응 단계
6-Methoxyisoquinoline (1.6 g) and benzyl bromide (2 ml) in acetone (75 ml) were heated under reflux for 1 hour. The mixture was diluted with ether and cooled to 0°. The solid was filtered off and recrystallised from methanol/ether, and had m.p. 155°-158°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04042697 |
| 출처 데이터셋 | uspto-grants-1977_08 |
| ORD ID | ord-a515023c47354e99bfa7c2376c17c423 |
| 출처 메모 | uspto-grants-1977_08 |