Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Chloro-2-nitrobenzoic acid → 5-Chloro-2-nitrobenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Chloro-2-nitrobenzoic acid | HCID 17286 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | 5-Chloro-2-nitrobenzoyl chloride | HCID 2723685 | 98% |
반응 단계
100.00 g (0.50 mol) of 5-chloro-2-nitrobenzoic acid were mixed with 72.20 g (0.61 mol) of thionyl chloride and the mixture was heated under reflux for 2 h. The excess thionyl chloride was removed in vacuo. 106.50 g (ca. 98%) of crude 5-chloro-2-nitro-benzoyl chloride were obtained as an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08541410B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-98241a4d407344f4a0ba01242af87eef |
| 출처 메모 | uspto-grants-2013_09 |