Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → 2-nitroethyl Acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | Benzene | HCID 241 | — |
| 반응물 | HCID 22056827 | HCID 22056827 | — |
| 촉매 | Sulfuric Acid | HCID 1118 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-nitroethyl Acetate | HCID 11815399 | — |
반응 단계
64 g nitroethanol, 50 ml glacial acetic acid, 250 ml benzene and 5 drops conc. H2SO4 were refluxed, using a water separator for 8 hours; 12 ml of H2O were collected. The solution was evaporated and vacuum distilled (1mm at 60° C) yielding 89 g colorless nitroethylacetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04044020 |
| 출처 데이터셋 | uspto-grants-1977_08 |
| ORD ID | ord-69984e74caad4c0abca1aeb28fb2ec24 |
| 출처 메모 | uspto-grants-1977_08 |