Azolimine → HCID 178482452, 화합물

HRID 442029노트

반응식

HRID 442029 반응식
[C:1]1([N:7]2[CH2:11][C:10](=[O:12])[N:9](C)[C:8]2=[NH:14])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:15][O-].[Na+]>>[C:1]1([N:7]2[CH2:11][C:10](=[O:12])[N:9]=[C:8]2[NH:14][CH3:15])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

참가 물질

3

반응물 2

HCID 38684AzolimineHCID 10942334Sodium Methoxide

생성물 1

HCID 178482452HCID 178482452, 화합물

실험 절차

2.2 g. of 1-phenyl-2-imino-3-methyl-4-oxoimidazolidine, 0.26 g. of sodium methoxide and 65 ml. of absolute alcohol were heated to reflux for 20 hours. The insoluble solid was filtered and ethanol was evaporated leaving a yellow solid.

후처리

  1. temperatureto reflux for 20 hours
  2. filtrationThe insoluble solid was filtered
  3. customethanol was evaporated
  4. customleaving a yellow solid

출처 및 근거

ORD 기록
ord-b99d745079f34d218d87641eb10ba8db
출처 데이터셋
uspto-grants-1977_08
특허 번호
US04044021

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