Thionyl Chloride → p-Chloromethylphenylacetyl chloride

HRID 442346

반응식

HRID 442346 반응식
[Cl:1][CH2:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][C:10]([OH:12])=O)=[CH:5][CH:4]=1.S(Cl)([Cl:15])=O>>[Cl:1][CH2:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][C:10]([Cl:15])=[O:12])=[CH:5][CH:4]=1

참가 물질

3

반응물 2

HCID 24386Thionyl Chloride2회HCID 103134194-(Chloromethyl)phenylacetic acid

생성물 1

HCID 20380233p-Chloromethylphenylacetyl chloride

실험 절차

A mixture of 1 g of p-chloromethylphenylacetic acid and 6 ml of thionyl chloride is stirred at room temperature for 25 hours after which the excess thionyl chloride is removed under vacuum to yield p-chloromethylphenylacetyl chloride.

후처리

  1. customis removed under vacuum

출처 및 근거

ORD 기록
ord-05a6d14492d4416e891aa8b6f6a8d12a
출처 데이터셋
uspto-grants-1977_08
특허 번호
US04045438

연결된 노트

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