Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Methyl-2-nitrobenzoic acid → 5-Methyl-2-nitrobenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Methyl-2-nitrobenzoic acid | HCID 18371 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | 5-Methyl-2-nitrobenzoyl chloride | HCID 3016013 | — |
반응 단계
A mixture of 5-methyl-2-nitrobenzoic acid (3.6 g, 19.87 mmol) and thionyl chloride (18 mL) was stirred under reflux for 20 hours then concentrated under reduced pressure to give 5-methyl-2-nitrobenzoyl chloride (3.77 g) which was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08541407B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-2380136c791e4cb694bce3db9ce279d8 |
| 출처 메모 | uspto-grants-2013_09 |