Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Ether → (1S)-1-Methyl-2-nitroxyethylamine hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| 반응물 | (1S)-N-(t-butoxycarbonyl)-1-methyl-2-nitroxyethylamine | HCID 45092343 | — |
| 생성물 | (1S)-1-Methyl-2-nitroxyethylamine hydrochloride | HCID 86754033 | — |
반응 단계
In 80 ml of 4N hydrochloric acid-dioxane were dissolved 4.52 g of (1S)-N-(t-butoxycarbonyl)-1-methyl-2-nitroxyethylamine, and the mixture was left to stand at room temperature for 1 hour and 50 minutes. To the mixture were added 160 ml of ether, and the crystals were collected by filtration and dried to obtain 3.02 g of the desired compound as colorless crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05891898 |
| 출처 데이터셋 | uspto-grants-1999_04 |
| ORD ID | ord-21634171d01d4347a88d48f984cf1d4f |
| 출처 메모 | uspto-grants-1999_04 |