Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Ethyl-1,3-Hexanediol → 2-Ethyl-1-triethoxysiloxy-3-hexanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Ethyl-1,3-Hexanediol | HCID 7211 | — |
| 반응물 | Dicyclohexylamine | HCID 7582 | — |
| 반응물 | Triethoxychlorosilane | HCID 78398 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Ethyl-1-triethoxysiloxy-3-hexanol | HCID 53757268 | 50% |
반응 단계
2-Ethyl-1,3-hexanediol was mixed with chlorotriethoxysilane and dicyclohexylamine in a 1:1:1 ratio at 0° C. in absolute ethanol. The resulting product, 2-ethyl-1-triethoxysiloxy-3-hexanol, was obtained in 50% yield and was dissolved to a 10% by weight solution in a 50/50 by volume mixture of ethanol/cyclomethicone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05891914 |
| 출처 데이터셋 | uspto-grants-1999_04 |
| ORD ID | ord-91f0fc7233b84088ae42805e4afe647b |
| 출처 메모 | uspto-grants-1999_04 |