Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 1-Triethoxysilylglycerol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Glycerol | HCID 753 | — |
| 반응물 | Dicyclohexylamine | HCID 7582 | — |
| 반응물 | Chlorosilane | HCID 61622 | — |
| 반응물 | Triethoxychlorosilane | HCID 78398 | — |
| 생성물 | 1-Triethoxysilylglycerol | HCID 54427112 | 90% |
반응 단계
Glycerol (GL) was reacted with chlorotriethoxysilane (CTS) in a 1:1 ratio at 0° C. in a 50/50 mixture of ethanol/cyclomethicone, using a 1:1 ratio of dicyclohexylamine to chlorosilane as the HCl scavenger. The resulting product, 1-triethoxysilylglycerol, was obtained in 90% yield and was dissolved to a 10% by weight solution in a 50/50 by volume mixture of ethanol/cyclomethicone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05891914 |
| 출처 데이터셋 | uspto-grants-1999_04 |
| ORD ID | ord-34a137cec1d84963b67a4990cd97ac55 |
| 출처 메모 | uspto-grants-1999_04 |