4,4'-Dichlorobenzhydrol → HCID 67594334, 화합물

HRID 442876

반응식

HRID 442876 반응식
[Cl:1][C:2]1[CH:16]=[CH:15][C:5]([CH:6](O)[C:7]2[CH:12]=[CH:11][C:10]([Cl:13])=[CH:9][CH:8]=2)=[CH:4][CH:3]=1.[CH:17]([NH:20][S:21]([C:24]1[NH:25][C:26]2[C:31]([CH:32]=1)=[CH:30][CH:29]=[CH:28][CH:27]=2)(=[O:23])=[O:22])([CH3:19])[CH3:18]>>[CH:17]([NH:20][S:21]([C:24]1[NH:25][C:26]2[C:31]([C:32]=1[CH:6]([C:7]1[CH:12]=[CH:11][C:10]([Cl:13])=[CH:9][CH:8]=1)[C:5]1[CH:15]=[CH:16][C:2]([Cl:1])=[CH:3][CH:4]=1)=[CH:30][CH:29]=[CH:28][CH:27]=2)(=[O:23])=[O:22])([CH3:19])[CH3:18]

참가 물질

3

반응물 2

HCID 70334,4'-DichlorobenzhydrolHCID 54122335N-isopropylindole-2-sulfonamide

생성물 1

HCID 67594334HCID 67594334, 화합물수율 83%

실험 절차

Substantially the same procedure as in Example 266 was repeated using 4,4'-dichlorobenzhydrol (1.14 g, 4.50 mmol) and N-isopropylindole-2-sulfonamide (1.00 g, 4.46 mmol) to give 1.76 g (yield: 83%-) of the title compound.

출처 및 근거

ORD 기록
ord-06f411ef2475488ab32e3eb30bb79182
출처 데이터셋
uspto-grants-1999_04
특허 번호
US05891902

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