Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N,N-Dimethylaniline → Carbofuran
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N,N-Dimethylaniline | HCID 949 | — |
| 반응물 | 1-Chloroethyl 2,3-dihydro-2,2-dimethyl-7-benzofuranyl carbonate | HCID 13557095 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | Carbofuran | HCID 2566 | — |
반응 단계
The procedure is as in (a) followed by (b), but pyridine is replaced by N,N-dimethylaniline and the intermediate carbonate is not distilled. Starting with 16.4 g of 2,3-dihydro-2,2-dimethyl-7-benzofuranol, 16.8 g (76%) of CARBOFURAN are then obtained, M.p. 147° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04725680 |
| 출처 데이터셋 | uspto-grants-1988_02 |
| ORD ID | ord-d4106ac42a79474482487a508c64ea90 |
| 출처 메모 | uspto-grants-1988_02 |