Methanol → 1H-Indole, 3-(methoxymethyl)-

HRID 443316노트

반응식

HRID 443316 반응식
[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]([CH2:10][OH:11])=[CH:2]1.[CH3:12]O>O>[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]([CH2:10][O:11][CH3:12])=[CH:2]1

참가 물질

4

반응물 2

HCID 887Methanol3회HCID 3712Indole-3-Carbinol

생성물 1

HCID 1544111H-Indole, 3-(methoxymethyl)-

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

Relatively pure 1H-indole-3-methanol (I3C™ from Designed Nutritional Products, Orem, UT, US) in a water solution was prepared for HPLC analysis. One sample was diluted with water and the other was diluted with methanol. By the time the partial methanol solution could be injected into the HPLC, the reaction with methanol had taken place to form 1H-indol-3-yl methoxy methane, the methyl ether of 1H-indole-3-methanol, and two peaks of about the same magnitude were observed. The same solution when diluted with water showed only one peak.

출처 및 근거

ORD 기록
ord-9c17ecac43234beeaadb3d6b3e14c901
출처 데이터셋
uspto-grants-1999_04
특허 번호
US05895787

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