Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoyl isocyanate → N-(3-Cyano-5-methylthiophen-2-ylcarbamoyl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoyl isocyanate | HCID 78210 | — |
| 반응물 | 2-Amino-5-methyl-3-thiophenecarbonitrile | HCID 689056 | — |
| 생성물 | N-(3-Cyano-5-methylthiophen-2-ylcarbamoyl)benzamide | HCID 57456905 | — |
반응 단계
Prepared as in Example 1a from 2-amino-5-methylthiophene-3-carbonitrile and benzoyl isocyanate as a white solid. 1H NMR (400 MHz, DMSO-d6) δ2.36 (d, J=1.2 Hz, 3H), 6.89 (d, J=1.2 Hz, 1H), 7.55 (t, J=8.0 Hz, 2H), 7.66 (d, J=7.2 Hz, 1H), 8.03-8.01 (m, 2H), 11.60 (brs, 1H), 12.08 (bs, 1H). MS 286 (MH+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08541421B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-5d25c90e84924c199e87f72d7d77db23 |
| 출처 메모 | uspto-grants-2013_09 |