4-Amino-1,2,4-triazole → 8-(2-Pyridyl)-1,2,4-triazolo[4,3-b]pyridazine

HRID 443520

반응식

HRID 443520 반응식
C[N:2](C)[CH:3]=[CH:4][C:5]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][N:8]=1)=O.N[N:15]1[CH:19]=[N:18][N:17]=[CH:16]1>C1(C)C(C)=CC=CC=1>[N:8]1[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=1[C:5]1[C:19]2[N:15]([CH:16]=[N:17][N:18]=2)[N:2]=[CH:3][CH:4]=1

참가 물질

4

반응물 2

HCID 114324-Amino-1,2,4-triazoleHCID 5669933-Dimethylamino-1-(2-pyridyl)prop-2-en-1-one

생성물 1

HCID 234675758-(2-Pyridyl)-1,2,4-triazolo[4,3-b]pyridazine

시약·촉매·용매 1

HCID 7237O-Xylene용매

실험 절차

As for Example 16, a mixture of 3-dimethylamino-1-(2-pyridyl)-2-propen-1-one, 4-amino-1,2,4-triazole and xylene is refluxed for 16 hours to give the product of the Example.

후처리

  1. temperatureis refluxed for 16 hours
  2. customto give the product of the Example

출처 및 근거

ORD 기록
ord-aebb5e9a5cc14393b4f4245b6d4c5e7b
출처 데이터셋
uspto-grants-1981_04
특허 번호
US04260756

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