4-Amino-1,2,4-triazole → 8-(2-Pyridyl)-1,2,4-triazolo[4,3-b]pyridazine

반응식

C[N:2](C)[CH:3]=[CH:4][C:5]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][N:8]=1)=O.N[N:15]1[CH:19]=[N:18][N:17]=[CH:16]1>C1(C)C(C)=CC=CC=1>[N:8]1[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=1[C:5]1[C:19]2[N:15]([CH:16]=[N:17][N:18]=2)[N:2]=[CH:3][CH:4]=1

참가 물질

실험 절차

As for Example 16, a mixture of 3-dimethylamino-1-(2-pyridyl)-2-propen-1-one, 4-amino-1,2,4-triazole and xylene is refluxed for 16 hours to give the product of the Example.

후처리

temperatureis refluxed for 16 hours
customto give the product of the Example

출처 및 근거

ORD 기록: ord-aebb5e9a5cc14393b4f4245b6d4c5e7b
출처 데이터셋: uspto-grants-1981_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04260756

반응 노트

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참가 물질

반응물 2

HCID 114324-Amino-1,2,4-triazole

HCID 5669933-Dimethylamino-1-(2-pyridyl)prop-2-en-1-one

생성물 1

HCID 234675758-(2-Pyridyl)-1,2,4-triazolo[4,3-b]pyridazine

시약·촉매·용매 1

HCID 7237O-Xylene용매

실험 절차

As for Example 16, a mixture of 3-dimethylamino-1-(2-pyridyl)-2-propen-1-one, 4-amino-1,2,4-triazole and xylene is refluxed for 16 hours to give the product of the Example.

후처리

temperatureis refluxed for 16 hours
customto give the product of the Example

출처 및 근거

ORD 기록: ord-aebb5e9a5cc14393b4f4245b6d4c5e7b
출처 데이터셋: uspto-grants-1981_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04260756

반응 노트

불러오는 중…