Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitrourea → Diethyl 2-(3-hydroxy-3-(p-biphenylyl)-propylamino)nonanedioate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitrourea | HCID 62372 | — |
| 반응물 | 1,4-Pentadien-3-one | HCID 543199 | — |
| 반응물 | Diethyl 2-(3-oxo-3-(p-biphenylyl)propylamino)nonanedioate | HCID 70578184 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Diethyl 2-(3-hydroxy-3-(p-biphenylyl)-propylamino)nonanedioate | HCID 70510532 | — |
반응 단계
A solution of diethyl 2-(3-hydroxy-3-(p-biphenylyl)-propylamino)nonanedioate (5 g), which was prepared via diethyl 2-(3-oxo-3-(p-biphenylyl)propylamino)nonanedioate from the appropriate vinyl ketone using the procedure of Example 2, in absolute ethanol (20 ml) was heated at 60° while nitrourea (1.12 g) was added portion-by-portion.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04262128 |
| 출처 데이터셋 | uspto-grants-1981_04 |
| ORD ID | ord-7d53ce85b93c416e9ea091733dd1cfec |
| 출처 메모 | uspto-grants-1981_04 |