Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 2,6-Di-tert-butyl-4-(chloromethyl)phenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Butylated hydroxymethylphenol | HCID 6929 | — |
| 용매 | Hexane | HCID 8058 | — |
| 생성물 | 2,6-Di-tert-butyl-4-(chloromethyl)phenol | HCID 12378601 | — |
반응 단계
176 grams of 4-hydroxy-3,5-di-tert-butyl-benzyl alcohol was slurried in 350 ml of hexane. 240 cc of concentrated HCl was added to the slurry and stirred overnight. The two phases were allowed to separate and the hexane phase washed twice with water. The dried hexane was then extracted with magnesium sulfate and filtered. Rotofilm evaporation yielded 168 grams of product--a pungent yellow liquid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04263154 |
| 출처 데이터셋 | uspto-grants-1981_04 |
| ORD ID | ord-0c6429c18bae40c796f71c081f89e807 |
| 출처 메모 | uspto-grants-1981_04 |