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Sodium Cyanide → HCID 23464477, 화합물

HRID 444167
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반응식

HRID 444167 반응식
Br[CH2:2][C:3]1[CH:18]=[CH:17][C:6]2[C:7](=[O:16])[NH:8][C:9]3[CH:15]=[CH:14][CH:13]=[CH:12][C:10]=3[S:11][C:5]=2[CH:4]=1.[C-:19]#[N:20].[Na+]>CN(C)C=O>[C:19]([CH2:2][C:3]1[CH:18]=[CH:17][C:6]2[C:7](=[O:16])[NH:8][C:9]3[CH:15]=[CH:14][CH:13]=[CH:12][C:10]=3[S:11][C:5]=2[CH:4]=1)#[N:20]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 8929Sodium CyanideHCID 23464491HCID 23464491, 화합물

생성물 1

HCID 23464477HCID 23464477, 화합물

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

Dissolve 6.4 gm. of the bromide of Step B in 75 cc. of dimethylformamide and add 2.95 gm. of sodium cyanide. Stir the mixture at room temperature for 1.5 hours. Dilute with 600 cc. of water and extract three times with ether. Wash the combined organics with water, dry and strip to a solid residue. Triturate in hexane and recover the solid by filtration.

후처리

  1. dissolutionDissolve 6.4 gm
  2. additionDilute with 600 cc
  3. extractionof water and extract three times with ether
  4. washWash the combined organics with water
  5. customdry
  6. customTriturate in hexane
  7. customrecover the solid
  8. filtrationby filtration

출처 및 근거

ORD 기록
ord-ef01500807144ce8b99c663e8e7dd45b
출처 데이터셋
uspto-grants-1981_04
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04263207

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