Dimethylamine → SBB061064

HRID 444188

반응식

HRID 444188 반응식
Cl[CH2:2][CH2:3][O:4][CH2:5][CH2:6][O:7][CH2:8][CH2:9][OH:10].[CH3:11][NH:12][CH3:13]>>[CH3:11][N:12]([CH3:13])[CH2:2][CH2:3][O:4][CH2:5][CH2:6][O:7][CH2:8][CH2:9][OH:10]

참가 물질

3

반응물 2

HCID 674DimethylamineHCID 788712-(2-(2-Chloroethoxy)ethoxy)ethanol

생성물 1

HCID 10845034SBB061064

실험 절차

Commercial Cl(CH2CH2O)3H (abb. ClE3H) (2.0 mole) and dimethylamine (20.0 mole) were mixed in a flask (3.0 l) fitted with a condenser and stirred (RT) for 30 hours. TLC (Si-gel) examination showed the complete consumption of the ClE3H. Excess dimethylamine was removed by two consecutive evaporations under reduced pressure. The residual material was reconstituted in CHCl3, dried (MgSO4), filtered and evaporated to dryness to produce the product, 8-dimethylamino-3,6-dioxaoctanol.

후처리

  1. customfitted with a condenser
  2. customthe complete consumption of the ClE3H
  3. customExcess dimethylamine was removed by two consecutive evaporations under reduced pressure
  4. dry with materialdried (MgSO4)
  5. filtrationfiltered
  6. customevaporated to dryness

출처 및 근거

ORD 기록
ord-640529c8258d4e74a8dd8c70eedc4121
출처 데이터셋
uspto-grants-1981_04
특허 번호
US04263281

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