Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → HCID 178479714, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | N-Phenylbenzimidoyl chloride | HCID 264587 | — |
| 반응물 | 2-[beta-(1-Pyrrolidinyl)ethylthio]phenol | HCID 23463674 | — |
| 생성물 | HCID 178479714 | HCID 178479714 | 55% |
반응 단계
A solution of 5.5 gms (0.025 mole) of 2-[β-(1-pyrrolidinyl)ethylthio]phenol and 5.3 gms (0.025 mole) of N-phenylbenzimidoyl chloride in 50 ml acetone was stirred at room temperature for a period of two hours. The desired product crystallized out. It was filtered, washed with acetone and dried at room temperature. Recrystallization from isopropanol yielded 6.0 gms (55%) of product, M.P. 167°-9° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04264505 |
| 출처 데이터셋 | uspto-grants-1981_04 |
| ORD ID | ord-ab2aae96cb804d669c17c205bc8864e3 |
| 출처 메모 | uspto-grants-1981_04 |