Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → (6-Methylpyridin-2-yl)methanol hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | (6-Methylpyridin-2-yl)methyl acetate | HCID 291137 | — |
| 생성물 | (6-Methylpyridin-2-yl)methanol hydrochloride | HCID 18413908 | — |
반응 단계
A solution of (6-methylpyridin-2-yl)methyl acetate (1.0 g) in concentrated HCl (3 mL) was refluxed for 1 h. The reaction mixture was then concentrated in vacuo to obtain the crude product. The crude material was azeotroped with toluene, and the residue obtained was filtered and dried in vacuo to afford (6-methylpyridin-2-yl)methanol hydrochloride (811 mg) as a solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08481534B2 |
| 출처 데이터셋 | uspto-grants-2013_07 |
| ORD ID | ord-fbf72e3296044ccb8ffa6a04d73dd71d |
| 출처 메모 | uspto-grants-2013_07 |