Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dichloromethane → HCID 57171531, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dichloromethane | HCID 6344 | — |
| 반응물 | Phenylboronic Acid | HCID 66827 | — |
| 반응물 | 4-Chloro-3-ethylphenol | HCID 84223 | — |
| 생성물 | HCID 57171531 | HCID 57171531 | — |
반응 단계
3-ethyl-4-chlorophenol (2.0 g, 0.013 mol), phenylboronic acid (4.7 g, 0.038 mol), TEA (11 mL, 0.077 mol), cupric acetate (4.2 g, 0.023 mol) and DCM (60 mL, 0.9 mol) were added to a 100 mL oven dried flask and the reaction was stirred at rt for 24 h. The solvent was then removed under reduced pressure and the resulting residue was purified by flash chromatography (5% EtOAc in Hexane).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08481733B2 |
| 출처 데이터셋 | uspto-grants-2013_07 |
| ORD ID | ord-468ee86025da4a8694d036ab3c535b72 |
| 출처 메모 | uspto-grants-2013_07 |