Adipic Acid → 6-(2,3-Dichlorophenyl)-1,2,4-triazine-3,5-diamine;hexanedioate

HRID 449791

반응식

HRID 449791 반응식
[CH:1]1[CH:6]=[C:5]([Cl:7])[C:4]([Cl:8])=[C:3]([C:9]2[N:14]=[N:13][C:12]([NH2:15])=[N:11][C:10]=2[NH2:16])[CH:2]=1.[C:17]([OH:26])(=[O:25])[CH2:18][CH2:19][CH2:20][CH2:21][C:22]([OH:24])=[O:23]>CO>[CH:1]1[CH:6]=[C:5]([Cl:7])[C:4]([Cl:8])=[C:3]([C:9]2[N:14]=[N:13][C:12]([NH2:15])=[N:11][C:10]=2[NH2:16])[CH:2]=1.[C:17]([O-:26])(=[O:25])[CH2:18][CH2:19][CH2:20][CH2:21][C:22]([O-:24])=[O:23]

참가 물질

4

반응물 2

HCID 196Adipic AcidHCID 3878Lamotrigine

생성물 1

HCID 866323226-(2,3-Dichlorophenyl)-1,2,4-triazine-3,5-diamine;hexanedioate

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

16 mg of lamotrigine was dissolved in 2 ml of methanol, 11 mg of adipic acid was added to the solution to form a single solution. The solution was then allowed to stand for several hours to effect the slow evaporation of solvent. The solids gathered were stored in screw cap vials for subsequent analysis.

후처리

  1. customto form a single solution
  2. waitto stand for several hours
  3. customthe slow evaporation of solvent
  4. customcap vials for subsequent analysis

출처 및 근거

ORD 기록
ord-9374823017d143f1a784e1a60c0199c4
출처 데이터셋
uspto-grants-2013_07
특허 번호
US08486927B2

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